Solutions Manual for A Small Scale Approach to Organic Laboratory Techniques 3rd Edition by Pavia Lampman Kriz and Engel

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Product Descriptions

Featuring new experiments, a new essay, and new coverage of nanotechnology, this organic chemistry laboratory textbook offers a comprehensive treatment of laboratory techniques including small scale and some microscale methods that use standard-scale (“macroscale”) glassware and equipment. The book is organized based on essays and topics of current interest and covers a large number of traditional organic reactions and syntheses, as well as experiments with a biological or health science focus. Seven introductory technique-based experiments, thirteen project-based experiments, and sections on green chemistry and biofuels spark students’ interest and engage them in the learning process. Instructors may choose to offer Cengage Learning’s optional Premium Website, which contains videos on basic organic laboratory techniques.

Table of Contents

Part 1: Introduction to Basic Laboratory Techniques
Experiment 1: Solubility
Experiment 2: Crystallization
Experiment 3: Extraction
Experiment 4: A Separation and Purification Scheme
Experiment 5: Chromatography
Experiment 6: Simple and Fractional Distillation
Experiment 7: Infrared Spectroscopy and Boiling-Point Determination
Experiment 8: Acetylsalicylic Acid
Experiment 9: Acetaminophen
Experiment 10: TLC Analysis of Analgesic Drugs
Experiment 11: Isolation of Caffeine from Tea Leaves
Experiment 12: Isopentyl Acetate (Banana Oil)
Experiment 13: Isolation of Eugenol from Cloves
Experiment 14: Spearmint and Caraway Oil: (+)- and (–)-Carvones
Experiment 15: Isolation of Chlorophyll and Carotenoid Pigments from Spinach
Experiment 16: Ethanol from Sucrose

Part 2: Introduction to Molecular Modeling
Experiment 17: An Introduction to Molecular Modeling
Experiment 18: Computational Chemistry

Part 3: Properties and Reactions of Organic Compounds
Experiment 19: Reactivities of Some Alkyl Halides
Experiment 20: Nucleophilic Substitution Reactions: Competing Nucleophiles
Experiment 21: Synthesis of n-Butyl Bromide and t-Pentyl Chloride
Experiment 22: 4-Methylcyclohexene
Experiment 23: Methyl Stearate from Methyl Oleate
Experiment 24: Gas-Chromatographic Analysis of Gasolines
Experiment 25: Biodiesel
Experiment 26: Ethanol from Corn
Experiment 27: Chiral Reduction of Ethyl Acetoacetate; Optical Purity Determination
Experiment 28: Nitration of Aromatic Compounds Using a Recyclable Catalyst
Experiment 29: Reduction of Ketones Using Carrots as Biological Reducing Agents
Experiment 30: Resolution of (±)-α-Phenylethylamine and Determination of Optical Purity
Experiment 31: An Oxidation–Reduction Scheme: Borneol, Camphor, Isoborneol
Experiment 32: Multistep Reaction Sequences: The Conversion of Benzaldehyde to Benzilic Acid
Experiment 33: Triphenylmethanol and Benzoic Acid
Experiment 34: Aqueous-Based Organozinc Reactions
Experiment 35: Sonogashira Coupling of Iodosubstituted Aromatic Compounds with Alkynes using a Palla
Experiment 36: Grubbs-Catalyzed Metathesis of Eugenol with 1,4-Butenediol to Prepare a Natural Produ
Experiment 37: The Aldol Condensation Reaction: Preparation of Benzalacetophenones (Chalcones)
Experiment 38: A Green Enantioselective Aldol Condensation Reaction
Experiment 39: Preparation of an α, β-Unsaturated Ketone via Michael and Aldol Condensation Reacti
Experiment 40: Preparation of Triphenylpyridine
Experiment 41: 1,4-Diphenyl-1,3-Butadiene
Experiment 42: Relative Reactivities of Several Aromatic Compounds
Experiment 43: Nitration of Methyl Benzoate
Experiment 44: Benzocaine
Experiment 45: N,N-Diethyl-m-toluamide: The Insect Repellent “OFF”
Experiment 46: Sulfa Drugs: Preparation of Sulfanilamide
Experiment 47: Preparation and Properties of Polymers: Polyester, Nylon, and Polystyrene
Experiment 48: Ring-Opening Metathesis Polymerization (ROMP) using a Grubbs Catalyst: a Three-Step S
Experiment 49: The Diels–Alder Reaction of Cyclopentadiene with Maleic Anhydride
Experiment 50: Diels-Alder Reaction with Anthracene-9 Methanol
Experiment 51: Photoreduction of Benzophenone and Rearrangement of Benzpinacol to Benzopinacolone
Experiment 52: Luminol
Experiment 53: Carbohydrates
Experiment 54: Analysis of a Diet Soft Drink by HPLC

Part 4: Identification of Organic Substances
Experiment 55: Identification of Unknowns

Part 5: Project-Based Experiments
Experiment 56: Preparation of a C-4 or C-5 Acetate Ester
Experiment 57: Isolation of Essential Oils from Allspice, Caraway, Cinnamon, Cloves, Cumin, Fennel,
Experiment 58: Competing Nucleophiles in SN1 and SN2 Reactions: Investigations Using 2-Pentanol and
Experiment 59: Friedel–Crafts Acylation
Experiment 60: The Analysis of Antihistamine Drugs by Gas Chromatography–Mass Spectrometry
Experiment 61: Carbonation of an Unknown Aromatic Halide
Experiment 62: The Aldehyde Enigma
Experiment 63: Synthesis of Substituted Chalcones: A Guided-Inquiry Experience
Experiment 64: Green Epoxidation of Chalcones
Experiment 65: Cyclopropanation of Chalcones
Experiment 66: Michael and Aldol Condensation Reactions
Experiment 67: Esterification Reactions of Vanillin: The Use of NMR to Determine a Structure
Experiment 68: An Oxidation Puzzle

Part 6: The Techniques
Technique 1: Laboratory Safety
Technique 2: The Laboratory Notebook, Calculations, and Laboratory Records
Technique 3: Laboratory Glassware: Care and Cleaning
Technique 4: How to Find Data for Compounds: Handbooks and Catalogs
Technique 5: Measurement of Volume and Weight
Technique 6: Heating and Cooling Methods
Technique 7: Reaction Methods
Technique 8: Filtration
Technique 9: Physical Constants of Solids: The Melting Point
Technique 10: Solubility
Technique 11: Crystallization: Purification of Solids
Technique 12: Extractions, Separations, and Drying Agents
Technique 13: Physical Constants of Liquids: The Boiling Point and Density
Technique 14: Simple Distillation
Technique 15: Fractional Distillation, Azeotropes
Technique 16: Vacuum Distillation, Manometers
Technique 17: Sublimation
Technique 18: Steam Distillation
Technique 19: Column Chromatography
Technique 20: Thin-Layer Chromatography
Technique 21: High-Performance Liquid Chromatography (HPLC)
Technique 22: Gas Chromatography
Technique 23: Polarimetry
Technique 24: Refractometry
Technique 25: Infrared Spectroscopy
Technique 26: Nuclear Magnetic Resonance Spectroscopy (Proton NMR)
Technique 27: Carbon-13 Nuclear Magnetic Resonance Spectroscopy
Technique 28: Mass Spectrometry
Technique 29: Guide to the Chemical Literature

Product Details

Language: English
ISBN-10: 1439049327
ISBN-13: 978-1439049327
ISBN-13: 9781439049327

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